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determination of tobramycin by reversed-phase ion-pair high performance liquid chromatography with a refractiveindex detector

Liang ZHU, Jingkang WANG

《化学科学与工程前沿(英文)》 2013年 第7卷 第3期   页码 322-328 doi: 10.1007/s11705-013-1348-z

摘要: A simple and direct method without a derivation step for routine analysis of tobramycin has been developed. This method used reversed-phase ion-pair high performance liquid chromatography (HPLC) with a refractive index (RI) detector and a C18 column which is stable at pH above 1.00. The presence of 4.50 mg·mL trifluoroacetic acid (TFA) in the mobile phase improved the protonation of tobramycin and the formation of ion-pairs, and thus reduced its hydrophility. This unique separation–detection combination showed good linearity with correlation coefficients 0.9996 in the concentration range of 0.25–2.50 mg·mL . The quantitation limit and detection limit were determined to be 0.23 mg·mL and 0.071 mg·mL , respectively. Tobramycin was recovered in 98.00%, 98.84% and 99.64% for tobramycin solutions at concentrations of 2.25 mg·mL , 1.50 mg·mL and 0.75 mg·mL , respectively. The relative standard deviations for six spiked samples ranged from 0.20% to 2.40%, indicating a good reproducibility of this method.

关键词: tobramycin     aminoglycoside     refractive index detector     high-performance liquid chromatography     ion-pairing    

Tetra-detector size exclusion chromatography characterization of molecular and solution properties of

Qingbin Guo,Sheng Chang

《环境科学与工程前沿(英文)》 2017年 第11卷 第2期 doi: 10.1007/s11783-017-0922-x

摘要: Tetra-detector HPSEC was evaluated for the SMP characterization Molecular weight and intrinsic viscosity of the SMP were characterized Specific viscosity and osmotic pressure of the SMP solution were studied Approach to analyze the concentration polarization of the SMP was discussed Characterization of the molecular properties of soluble microbial products (SMP) is critical for understanding the membrane filtration and fouling mechanisms in anaerobic and aerobic membrane bioreactors (AnMBR & MBR). In this study, the distributions of the absolute molecular weight and intrinsic viscosity of SMP polysaccharides from an AnMBR were effectively determined by a high performance size exclusion chromatography (HPSEC) that was coupled with the refractive index (RI), diode array UV (DAUV), right and low angle light scattering (LS), and viscometer (Vis) detectors. Based on the tetra-detector HPSEC determined absolute molecular weights and intrinsic viscosity, a universal calibration relationship for the SMP polysaccharides was developed and the molecular conformations, average molecular weights, and hydrodynamic sizes of the SMP polysaccharides were also explored. Two factors which can be derived from the tetra-detector HPSEC analysis were proposed for the characterization of the viscous and osmotic pressure properties of the SMP polysaccharides. In addition, it was also extrapolated how to analyze the resistance characteristics of the concentration polarization layers formed in membrane filtration based on the molecular properties determined by the tetra-detector HPSEC analysis.

关键词: Soluble microbial product     Extracellular polymeric substance     Membrane bioreactor     Membrane fouling     Molecular weight     Intrinsic viscosity    

全静压受感器冰风洞试验技术研究

彭又新,郑莉,林贵平

《中国工程科学》 2009年 第11卷 第11期   页码 51-55

摘要:

主要论述了全静压受感器的冰风洞试验技术,着重介绍了该仪器的冰风洞试验项目、试验条件及参数测量校准方法,并从航空仪器仪表公司的冰风洞的自身特点出发,论述了该仪器冰风洞试验的效果及据此提出的改进建议,为今后国内对相应的小型仪器仪表或缩比模型进行冰风洞试验提供了一定的参考价值。

关键词: 全静压受感器     冰风洞试验     防冰    

The relevance of James Lovelock’s research and philosophy to environmental science and academia

《环境科学与工程前沿(英文)》 2023年 第17卷 第3期 doi: 10.1007/s11783-023-1639-7

摘要: James E. Lovelock, famed for his Gaia hypothesis, which views the Earth as a living integrated and interconnected self-regulating system whose equilibrium comes about from complex energy-based interactions and feedback loops, ultimately sustaining life, passed away at the end of July, 2022 at the age of 103. Not only are the adaptive mechanisms of Gaia central to the conversation of environmental homeostasis, they lie at the heart of climate change and global warming. Lovelock is also remembered as the co-inventor of the electron capture detector that eventually allowed for the sensitive detection of chlorofluorocarbons and pesticides. Finally, Lovelock’s free-spirited nature and research independence allow academia to rethink current research’s modus operandi.

关键词: Academic independence     Climate change     Electron capture detector     Environmental equilibrium     Global warming     Homeostasis    

Research on port ecological suitability evaluation index system and evaluation model

Yaofeng XIE,Xia LV,Ru LIU,Liuyan MAO,Xiaoxi LIU

《结构与土木工程前沿(英文)》 2015年 第9卷 第1期   页码 65-70 doi: 10.1007/s11709-014-0258-6

摘要: Along with the rapid development of port building, the negative impacts of port’s construction and operation on the coastline ecosystem are also increasingly strong. Therefore, it’s urgent to establish a scientific and complete system of port ecological suitability evaluation. This paper pointed out the characteristics of port ecological effects and the principles of selecting evaluation index, and used the “pressure-state-response (PSR)” model to analysis the various pressures on the environment caused by port construction and operation, and the system’s response. On this basis, we constructed the port ecological suitability evaluation index. This model used the combination of qualitative and quantitative analytic hierarchy process, to meet the multi-level, multi-objective characteristics of evaluation index system. The evaluation index system and evaluation model can be used to analysis the ecological suitability of port projects comprehensively and have some guiding significance to the port ecological suitability evaluation.

关键词: port     ecological suitability     press-state-response (PSR) model     evaluation index system    

A total torque index for dynamic performance evaluation of a radial symmetric six-legged robot

Kejia LI, Xilun DING, Marco CECCARELL

《机械工程前沿(英文)》 2012年 第7卷 第2期   页码 219-230 doi: 10.1007/s11465-012-0320-9

摘要:

This article focuses on the dynamic index and performance of a radial symmetric six-legged robot. At first the structure of the robot is described in brief and its inverse kinematics is presented. Then the dynamic model is formulated as based on the Lagrange equations. A novel index of total torque is proposed by considering the posture of the supporting legs. The new index can be used to optimize the leg’s structure and operation for consuming minimum power and avoiding unstable postures of the robot. A characterization of the proposed six-legged robot is obtained by a parametric analysis of robot performance through simulation using the presented dynamic model. Main influences are outlined as well as the usefulness of the proposed performance index.

关键词: six-legged robots     dynamic modeling     performance index    

Isolating higher yielding and more stable rice genotypes in stress environments: fine-tuning a selection method using production and resilience score indices

《农业科学与工程前沿(英文)》 doi: 10.15302/J-FASE-2023521

摘要:

● Score index methods readily discriminate genotypes adapted to a target environment.

关键词: Aerobic rice     breeding selection     drought resilience     production capacity index     resilience capacity index     stress score index     upland    

SUSTAINABLE NITROGEN MANAGEMENT INDEX: DEFINITION, GLOBAL ASSESSMENT AND POTENTIAL IMPROVEMENTS

《农业科学与工程前沿(英文)》 2022年 第9卷 第3期   页码 356-365 doi: 10.15302/J-FASE-2022458

摘要:

● A composite N management index is proposed to measure agriculture sustainability.

关键词: global assessment     indicator     nitrogen management     sustainable agriculture     sustainable development goals    

A novel power system reconfiguration for a distribution system with minimum load balancing index using

K. Sathish KUMAR, T. JAYABARATHI

《能源前沿(英文)》 2012年 第6卷 第3期   页码 260-265 doi: 10.1007/s11708-012-0196-8

摘要: In this paper, the objective of minimum load balancing index (LBI) for the 16-bus distribution system is achieved using bacterial foraging optimization algorithm (BFOA). The feeder reconfiguration problem is formulated as a non-linear optimization problem and the optimal solution is obtained using BFOA. With the proposed reconfiguration method, the radial structure of the distribution system is retained and the burden on the optimization technique is reduced. Test results are presented for the 16-bus sample network, the proposed reconfiguration method has effectively decreased the LBI, and the BFOA technique is efficient in searching for the optimal solution.

关键词: bacterial foraging optimization algorithm (BFOA)     distribution system     network reconfiguration     load balancing index (LBI)     radial network    

The Building of Papermaking Enterprise’s Recycling Economy Evaluation Index System Based on Value Flow

Zhi-fang Zhou,Jing Ou,Sha-sha Wang,Xiao-hong Chen

《工程管理前沿(英文)》 2016年 第3卷 第1期   页码 9-17 doi: 10.15302/J-FEM-2016009

摘要: At present, the research on circular economy has made a lot of substantive results both at home and abroad. But for the papermaking enterprise, which is the representative of the light industry, few studies have analyzed the evaluation index system of circular economy. Since the current material flow analyses have limitations that the researchers cannot calculate materials with different units. The authors take advantage of the intrinsic correlation between the basic principle of value flow analysis and circular economy, and then analyze the dynamic changes of material flow and value flow through enterprises internal production process. Considering the resource output, the authors set up the layered structure of the evaluation index system, and then preliminarily determine the index form. Next, the authors use the frequency statistics analysis method to adjust indicators, forming a preliminary index system. After that, the principal component analysis and independent analysis are applied for screening. Finally, the authors build a circular economy evaluation index system for papermaking enterprise to provide scientific guidance for the process of circular economy.

关键词: circular economy     the papermaking enterprise     material flow analysis     value flow analysis     evaluation index system    

Can the Shanghai LNG Price Index indicate Chinese market?

Yeli ZENG, Cong DONG, Mikael HÖÖK, Jinhua SUN, Danyang SHI

《能源前沿(英文)》 2020年 第14卷 第4期   页码 726-739 doi: 10.1007/s11708-020-0701-4

摘要: China became the world’s second largest liquefied natural gas (LNG) importer in 2018 but has faced extremely high import costs due to a lack of bargaining power. Assessments of the Shanghai LNG Price Index, first released in 2015, are vital for improving the understanding of these cost dynamics. This paper, using the LNG price index data from the Shanghai Petroleum and Gas Exchange (SHPGX) coupled with domestic and international LNG prices from July 1, 2015 to December 31, 2018, estimates several econometric models to evaluate the long-term and short-term equilibriums of the Shanghai LNG Price Index, the responses to market information shocks and the leading or lagging relationships with LNG and alternative energy prices from other agencies. The results show that the LNG price index of the SHPGX has already exhibited a long-term equilibrium and short-term adjustment mechanisms to reflect the average price level and market movements, but the market information transparency and price discovery efficiency of the index are still inadequate. China’s LNG market is still relatively independent of other natural gas markets, and marketization reforms are under way in China. The influence of the SHPGX LNG price index on the trading decisions of market participants is expected to improve with further development of China’s LNG reforms, the formation of a natural gas entry-exit system, and the increasing liquidity of the hub.

关键词: liquefied natural gas     price index     Shanghai Petroleum and Gas Exchange     price discovery     market reforms    

“制造强国”评价指标体系优化与测评研究

赵蔷,吴进军,夏鹏,王迪,刘丹,刘云,董晗

《中国工程科学》 2017年 第19卷 第3期   页码 13-19 doi: 10.15302/J-SSCAE-2017.03.003

摘要:

本文围绕制造强国指标体系数据源、计算方式、指标归类等方面进行了完善优化研究,持续开展了年度指数测评工作及指数背后制造业发展态势的深入剖析。同时对2016年制造强国综合指数进行了预测算,总结了近五年的发展趋势,为制造强国发展进程提供了有益的参考。

关键词: 指标体系     完善优化     指数测评     差距及瓶颈分析    

基于沃尔什特征的增强型AdaBoost 人脸快速检测算法

郭志波,杨静宇,刘华军,严云洋

《中国工程科学》 2008年 第10卷 第7期   页码 125-131

摘要:

提出一种基于沃尔什特征的增强型AdaBoost 人脸快速检测算法,不仅具有很快的训练速度,而且利 用较少的非人脸样本进行训练就可以达到较好的检测效果。首先,提出用较少的沃尔什特征来代替大量的 Harr-Like 特征可以较大幅度的降低特征之间的冗余。然后提出一种双阈值增强型AdaBoost 算法,其中双阈 值的快速搜索方法大大节约了训练时间,并且在训练Cascaded 检测器过程中,前层分类器的训练结果对后层 分类器的训练具有指导作用,加强了总体检测器的性能,另外通过各层分类器阈值的调节,能够将人脸和非 人脸的训练结果尽量分离。最后,使用该算法训练的检测器对MIT+CMU 人脸测试库进行了测试,结果表明 该方法在训练速度、测试精度、检测时间等方面都优于相应的方法。

关键词: 沃尔什特征     增强型AdaBoost     Cascaded 型检测器     人脸检测    

制造质量强国指标体系研究

郑立伟,张纲,蒋家东,王赟松

《中国工程科学》 2015年 第17卷 第7期   页码 76-75

摘要:

本文构建了制造质量强国指标体系,分为质量安全、质量发展和质量基础三个维度,建立了11个评价指标。通过实证分析将我国制造业产品质量与部分国家进行了比较,并分析了我国制造业质量水平变化的趋势。结论表明:我国制造业质量经历了一个稳步提升的过程,2008年金融危机后提升幅度明显下降;与新兴制造国家相比,我国产品质量表现出一定优势;与发达国家相比,仍存在安全、性能差距,影响了我国制造业的出口贸易。

关键词: 制造强国     质量评价     指标体系    

Pavement sustainability index for highway infrastructures: A case study of Maryland

Stella O. OBAZEE-IGBINEDION, Oludare OWOLABI

《结构与土木工程前沿(英文)》 2018年 第12卷 第2期   页码 192-200 doi: 10.1007/s11709-017-0413-y

摘要: Pavement deterioration creates conditions that undermine their performances, which gives rise to the need for maintenance and rehabilitation. This paper develops a mathematical multi-linear regression analysis (MLRA) model to determine a pavement sustainability index ( ) as dependent variable for flexible pavements in Maryland. Four categories of pavement performance evaluation indicators are subdivided into seven pavement condition indices and analyzed as independent variables for each section of pavement. Data are collected from five different roadways using field evaluations and existing database. Results indicate that coefficient of determination ( ) is correlated and significant, = 0.959. Of the seven independent variables, present serviceability index ( ) is the most significant with a coefficient value of 0.032, present serviceability rating ( ) coefficient value= 0.028, and international roughness index ( ) coefficient value= ?0.001. Increasing each unit value of coefficients for and would increase the value of ; thereby providing a more sustainable pavement infrastructure; which explains the significance of the model and why will most likely impact environmental, economic and social values.

关键词: pavement indices     sustainability     pavement performance     flexible pavements    

标题 作者 时间 类型 操作

determination of tobramycin by reversed-phase ion-pair high performance liquid chromatography with a refractiveindex detector

Liang ZHU, Jingkang WANG

期刊论文

Tetra-detector size exclusion chromatography characterization of molecular and solution properties of

Qingbin Guo,Sheng Chang

期刊论文

全静压受感器冰风洞试验技术研究

彭又新,郑莉,林贵平

期刊论文

The relevance of James Lovelock’s research and philosophy to environmental science and academia

期刊论文

Research on port ecological suitability evaluation index system and evaluation model

Yaofeng XIE,Xia LV,Ru LIU,Liuyan MAO,Xiaoxi LIU

期刊论文

A total torque index for dynamic performance evaluation of a radial symmetric six-legged robot

Kejia LI, Xilun DING, Marco CECCARELL

期刊论文

Isolating higher yielding and more stable rice genotypes in stress environments: fine-tuning a selection method using production and resilience score indices

期刊论文

SUSTAINABLE NITROGEN MANAGEMENT INDEX: DEFINITION, GLOBAL ASSESSMENT AND POTENTIAL IMPROVEMENTS

期刊论文

A novel power system reconfiguration for a distribution system with minimum load balancing index using

K. Sathish KUMAR, T. JAYABARATHI

期刊论文

The Building of Papermaking Enterprise’s Recycling Economy Evaluation Index System Based on Value Flow

Zhi-fang Zhou,Jing Ou,Sha-sha Wang,Xiao-hong Chen

期刊论文

Can the Shanghai LNG Price Index indicate Chinese market?

Yeli ZENG, Cong DONG, Mikael HÖÖK, Jinhua SUN, Danyang SHI

期刊论文

“制造强国”评价指标体系优化与测评研究

赵蔷,吴进军,夏鹏,王迪,刘丹,刘云,董晗

期刊论文

基于沃尔什特征的增强型AdaBoost 人脸快速检测算法

郭志波,杨静宇,刘华军,严云洋

期刊论文

制造质量强国指标体系研究

郑立伟,张纲,蒋家东,王赟松

期刊论文

Pavement sustainability index for highway infrastructures: A case study of Maryland

Stella O. OBAZEE-IGBINEDION, Oludare OWOLABI

期刊论文